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MOSINTER GROUP LIMITED
MOSINTER GROUP LIMITED

China P Toluene Sulfonic Amide CAS 70-55-3 PTSA manufacturer

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P Toluene Sulfonic Amide CAS 70-55-3 PTSA 

Payment Terms: T/T,L/C,WU 
Place of Origin: Sichuan, China (Mainland) 
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Product Detail

Means of Transport: Ocean,Land,Air
Packing: According to customer requi...
Brand Name: MOSINTER
Brand: MOSINTER
Molecular mass: 171.22
Melting point: 136-140℃
solubleness: 0.32 g/100 mL (25℃)
Production Capacity: 6000T/Year
Delivery Date: within 7 days
CAS No.: 70-55-3
Molecular Formula: C7H9NO2S
Density: 1.271g/cm3
Boiling point: 322.2℃ at 760 mmHg
Alias: PTSA

Used in organic synthesis. For toluene sulfonamide is mainly used for synthesis of chloramine -t and tolbutamide chloramphenicol (Tevenel).

P Toluene Sulfonic Amide(CAS: 70-55-3)


Item

Index

Appearance

White crystalline   powder

Melting point

136-140οC

Boiling point:

221οC

Flash point

202οC

Assay

 ≥99.5%

Moisture

≤0.1%

o-Toluene Sulfonamide

≤0.2%

Color(APHA)

≤20

Storage method 

  1. With inner plastic bags, outer woven bag or inner, middle, with a brown paper bag, plastic bags of outer woven bag packing. Stored in light with light, moisture, heat. According to provisions of flammable toxic substances are stored.

  2. This product should be kept sealed a cool and dry.

synthetic method

  1. By p-toluene sulfonyl chloride and ammonia reaction. Process: first to amination pot add just the right amount of ice water, then according to the ratio of quality (p-toluene sulfonyl chloride: pure ammonia = 1-0. 2) measuring good p-toluene sulfonyl chloride and ammonia in turn into the pot, to start the mixer, using amination pan pan jacketed cooling fluid control of temperature to 70 ℃ or so (the mass exothermic reaction, and then cooled to discharge is about 30 ℃. Amine compound into the filter barrels, wash with warm water and blot is solid powder products of toluene sulfonamide. Crude products of toluene sulfonamide contains a small amount of by-product ortho body letter oily non-ferrous material. By using the properties of para amine soluble in sodium hydroxide solution and using active carbon decoloring, can achieve purification refined. Ratio of material quality for coarse registration amine: 30% sodium hydroxide liquid alkali: water = 100:00 aroused; Coarse registration amine: activated carbon = 100: (2.5 3.5). According to the formula of the water and caustic soda in the purification of the pot, open the jacket steam valve heated to 70 ℃, then add.

  2. P-toluene sulfonyl chloride with pure ammonia, in turn, add to the ice water, control p-toluene sulfonyl chloride and pure ammonia quality ratio is 1:0.2, under stirring reaction, cooling and control the temperature of 70 ℃. After the reaction, cooling, filtering, washing products, products by caustic washing, bleaching, washing, neutralization, filtration, washing, drying for a quick finished products.

Application

1. Used in organic synthesis. For toluene sulfonamide is mainly used for synthesis of chloramine -t and tolbutamide chloramphenicol (Tevenel).

2. Used in the synthesis of fluorescent dye, plasticizer, synthetic resin, paint, disinfectants and wood processing brightener, etc. 

3. Mainly used for synthesis of water-soluble melamine formaldehyde resin toughening agent.

4. As a primary brightener in the bright nickel plating. Used for light multilayer nickel plating, uniform coating light. General dosage of 0.2 ~ 0.3 g/L.

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Company Info

MOSINTER GROUP LIMITED [China (Mainland)]

sgs ico Offline Showroom in USA

Business Type:Manufacturer, Trading Company
City: Ningbo
Province/State: Zhejiang
Country/Region: China (Mainland)

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